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Katayama, Yoshinori; Inamura, Yasuhiro*
Nuclear Instruments and Methods in Physics Research B, 238(1-4), p.154 - 159, 2005/08
Times Cited Count：8 Percentile：52.8(Instruments & Instrumentation)It is well know that many substances have different structures in the crystalline state and they exhibit first-order structural phase transitions by a change in pressure. On the other hand, pressure-induced structural changes in the liquid and glassy states were supposed to be monotonous. The recent development of synchrotron radiation sources enables us to perform structural studies on liquids and glasses under high pressure and high temperature conditions. These studies revealed that the changes in the liquid and glassy states are not necessarily monotonous. We will present recent results on liquid phosphorus and silica glass.
Sakaba, Nariaki; Tachibana, Yukio; Nakagawa, Shigeaki; Hamamoto, Shimpei
Transactions of 18th International Conference on Structural Mechanics in Reactor Technology (SMiRT-18), p.4499 - 4511, 2005/08
Safety demonstration tests using the HTTR are now underway in order to verify the inherent safety features and to improve the safety design and evaluation technologies for HTGRs, as well as to contribute to research and development for the VHTR, which is one of the Generation IV reactor candidates. The coolant flow reduction test by running down gas circulators, which is one of the safety demonstration tests, is a simulation test of anticipated transients without scram. During the coolant flow reduction test, temperature of the high-temperature helium components and chemistry in the primary circuit are changed rapidly. This paper describes the structural integrity assessments of helium components, e.g. helium pipes, heat exchangers, during the coolant flow reduction test. From the result of this evaluation, it was found that the helium components were kept their structural integrity during temperature and chemistry transient condition in the coolant flow reduction test from the reactor power at 30%. It was also confirmed by this assessment that the coolant flow reduction test will be able to perform with its enough safety margins from the reactor power at 100%.
resolutionChatake, Toshiyuki*; Kurihara, Kazuo; Tanaka, Ichiro*; Tsyba, I.*; Bau, R.*; Jenney, F. E. Jr.*; Adams, M. W. W.*; Niimura, Nobuo
Acta Crystallographica Section D, 60(8), p.1364 - 1373, 2004/08
Times Cited Count：34 Percentile：88.87(Biochemical Research Methods)A neutron diffraction study has been carried out at 1.6 resolution on a mutant rubredoxin from 
using the BIX-3 single-crystal diffractometer at the JRR-3 reactor of JAERI. In order to study the unusual thermostability of rubredoxin from 
, the hydrogen-bonding patterns were compared between the native and a 'triple-mutant' variant where three residues were changed so that they are identical to those in a mesophilic rubredoxin. In the present study, some minor changes were found between the wild-type and mutant proteins in the hydrogen-bonding patterns of the Trp3/Tyr3 region. The H/D-exchange ratios in the protein were also studied. The results suggest that the backbone amide bonds near the four Cys residues of the FeS
redox center are most resistant to H/D exchange. In addition, the 1.6 resolution of the present neutron structure determination has revealed a more detailed picture than previously available of some portions of the water structure, including ordered and disordered O-D bonds.
by BIX-3, a single-crystal diffractometer for biomacromoleculesKurihara, Kazuo; Tanaka, Ichiro*; Chatake, Toshiyuki*; Adams, M. W. W.*; Jenney, F. E. Jr.*; Moiseeva, N.*; Bau, R.*; Niimura, Nobuo
Proceedings of the National Academy of Sciences of the United States of America, 101(31), p.11215 - 11220, 2004/08
Times Cited Count：48 Percentile：61.07(Multidisciplinary Sciences)The structure of a rubredoxin (Rd) from , an organism that grows optimally at 100 
C, was determined using the neutron single-crystal diffractometer for biological macromolecules (BIX-3) at the JRR-3 reactor of JAERI. Data were collected at room temperature up to a resolution of 1.5 , and the completeness of the data set was 81.9 %. The model contains 306 H atoms and 50 D atoms. A total of 37 hydration water molecules were identified. The model has been refined to final agreement factors of 
= 18.6 % and 
= 21.7 %. Several orientations of the O-D bonds of side chains, whose assignments from X-ray data were previously ambiguous, were clearly visible in the neutron structure. While most backbone N-H bonds had undergone some degree of H/D exchange throughout the molecule, five H atom positions still had distinctly negative (H) peaks. The neutron Fourier maps clearly showed the details of an extensive set of H bonds involving the ND
terminus that may contribute to the unusual thermostability of this molecule.
Takeda, Takeshi; Tachibana, Yukio; Nakagawa, Shigeaki
JAERI-Tech 2002-091, 45 Pages, 2002/12
JAERI-Tech-2002-091.pdf:1.77MB
no abstracts in English
Terasaki, Hidenori*; Kato, Takumi*; Urakawa, Satoru*; Funakoshi, Kenichi*; Sato, Kiminori*; Suzuki, Akio*; Okada, Taku
Geophysical Research Letters, 29(8), p.68_1 - 68_3, 2002/05
The in situ viscosity measurements of the pure molten Fe under high pressures were made by falling sphere X-ray radiography method. Viscosity coefficients at about 2000 K were 15-24 mPa s at 2.7-5.0 GPa, and 4-9 mPa s at 5.0-7.0 GPa. Drastic decrease was found at around 5 GPa, at which stable solid phase below the melting temperatures change from delta (bcc) to gamma (fcc) phases. The observation indicates the possibility that the structural change in the molten Fe occurs in a narrow pressure interval (1 GPa) at the similar condition with the phase transformation in the solid.
Kurihara, Kazuo; Tanaka, Ichiro; Adams, M. W. W.*; Jenney, F. E. Jr.*; Moiseeva, N.*; Bau, R.*; Niimura, Nobuo
Journal of the Physical Society of Japan, Vol.70, Supplement A, p.400 - 402, 2001/05
With the new single-crystal diffractometer BIX-3 at the JRR-3M reactor of JAERI, a single-crystal neutron diffraction analysis of the structure of the small protein rubredoxin from the hyperthermophile Pyrococcus furiosus is currently under way. Data were collected at room temperature up to a resolution of 1.5 
intervals in 
and exposure times ranging from 60 to 77 minutes per frame. The completeness factor of the 1.5-
. Included in the refinement are 301 hydrogen atoms and 40 deuterium atoms, and 29 water molecules were also identified. In the present model, the current value for R and R
are 24.0 
and 26.3 , respectively.
Hada, Kazuhiko; Nishiguchi, Isoharu; ; Tsuji, Hirokazu
Nucl. Eng. Des., 132, p.1 - 11, 1991/00
Times Cited Count：24 Percentile：90.25(Nuclear Science & Technology)no abstracts in English
Tachibana, Yukio
no journal, ,
Japan Atomic Energy Agency (JAEA) has started the development of a domestic demonstration reactor based on the results of R&D activities conducted so far. In this presentation, an overview of the HTGR project, materials and operating conditions of HTTR high-temperature components will be presented, especially focusing on the development of intermediate heat exchangers and Hastelloy XR, and high-temperature structural design guidelines for HTGR Class 1 components will be introduced. In addition, future issues will be discussed.
